Ask an Expert
Charles Ross & Son prides itself on providing the most accurate and in depth knowledge for mixing and blending technology. Our engineers and manufacturing experts are readily available to answer any questions you may have about your process and equipment. With our "Ask an Expert" form, we can pass your questions directly along to our engineers for their insight and feedback. Below, you'll find a cumulative list of common questions, along with our answers.
View Popular Questions and Answers
Can single-stage rotor/stator mixers produce fine dispersions and emulsions with submicron particles or droplets?
Yes, standard high shear mixers are capable of producing submicron droplets or particles. But in large part, this is also highly dependent on the formulation itself. Apart from mixing intensity, several other factors affect particle or droplet size reduction including inherent properties of the raw materials, their interaction or chemistry, presence and type of surfactant, operating temperature, shear-sensitivity, etc. For this reason, particle size distribution can only be accurately determined through mixer trials wherein the actual raw materials are used and real process line conditions are simulated as closely as possible. In certain cases, even the same raw material sourced from a different supplier can yield significantly different results.
What would be a good mixer for protein powder and other dry powders?
There are many factors we are considering when assessing the best candidate for a dry blending project. The three most common choices are our Ribbon Blender, Tumble Blender, or Vertical Blender. Each design will have specific advantages in certain processes. For example, if there are ingredients in the blend that are a small percentage of the total batch, the Tumble Blender will have an advantage over the other two candidates. If large volumes are required and the ingredients are in similar percentages in the formulation, the ribbon blender will have the advantage. The Vertical Blender would likely be the best choice if heating or vacuum is an essential part of the blending process. For further information please watch our webinar titled, "A Ribbon, Tumble or Vertical Blender- Which is Best for My Process."
I am trying to disperse Carbon black pigment in wax but the dispersion is very poor. What equipment would you recommend?
There are several primary factors we consider in our effort to identify the best mixer candidate. The viscosity and the density of the material are among the most important factors to consider. Selecting a device that can provide an increased level of shear energy to the dispersion is likely to solve the problem. There are also other factors to consider as well. For example, vacuum mixing or mixing at an elevated temperature may be beneficial to generating the appropriate dispersion. Once the best candidates are identified, testing their performance with the product is a critical step in confirming the mixer selection is appropriate.
We have been developing a process on a bench-top scale. Could you help us with scaling up this process for production volumes?
Yes we can. We are commonly helping clients in this particular situation. We will evaluate and identify the critical process requirements and use that date to specify what is required to meet your production demands.
I am getting separation in my emulsion when making full scale batches. I don't see this separation with laboratory scale batches even though it is the same formulation. What am I doing wrong?
Emulsion separation in this situation is usually a result of insufficient shear energy to generate the appropriate droplet size. Looking at both the peak shear energy and the total energy per unit mass of product are two critical factors in generating the appropriate emulsion.
We would like to reduce our batch cycle time, what is the best way to accomplish this?
We need to first determine what the rate limiting step in the process is. In some applications, it may be the amount of mixing energy required to create the appropriate dispersion. This can be solved by adding an additional agitator, or swapping the existing agitator for one offering higher shear intensity.
My product is moisture sensitive. How can I minimize the introduction of water to the batch, especially on days with high humidity?
Processing in a mixer under vacuum or with a suitable nitrogen blanket are the best way to ensure no additional moisture from the atmosphere will be introduced to the product. Raw materials, especially hygroscopic solids, should be stored in an area that is free from moisture.
What improvements can vacuum mixing offer to product quality?
Vacuum mixing offers several advantages that can enhance product quality. It eliminates entrained air, including moisture and oxygen, which can negatively impact product stability and shelf life. Vacuum mixing often improves appearance and improves the dispersion of solids in the final product. These characteristics make vacuum mixing a preferred choice for applications requiring high-quality and stable products.
What type of high shear mixer can handle non-Newtonian fluids which will "harden" as shear is introduced.
For dilatant materials, high shear can be generated with relatively low velocity, depending on the characteristics of your particular fluid.
Planetary Mixers and Multi-shaft Mixers are commonly utilized in applications where we see this fluid behavior. We rarely see rotor/ stator mixers for applications involving dilatant materials.
Can the Vertical Blender be mounted on load cells and used as a weighing device?
Yes, the Vertical Blender can be mounted on load cells and used as a weighing device.
What is the minimum working capacity in a VCB tumble blender?
A: The minimum batch on a VCB tumble blender will depend largely on whether you are using an intensifier bar. When considering just the mixing aspect without an intensifier bar, 1/10 of the working volume could be mixed. If using an intensifier bar, you would have to select a batch height where the product sufficiently contacts the high speed blades.
How can we reduce foaming during mixing of surfactants?
When mixing liquids that are prone to generating foam, you should look to minimize turbulence at the surface of the batch. This includes avoiding top entering agitators if they run at an appreciable speed. Low speed, anchor agitators can be utilized if the agitator is relatively large in diameter and running at a slow rotational speed.
Are ROSS Mixers 21 CFR Part 11 compliant?
Title 21 CFR Part 11 are regulations pertaining to records in electronic form that are created, modified, maintained, archived, retrieved, and/or transmitted under any records requirement set forth by the FDA. ROSS Mixers can be supplied with a data acquisition software package compliant with 21 CFR Part 11, ensuring that electronic records and signatures are considered trustworthy, reliable and equivalent to paper records.
Will I be able to achieve a product with less than 1% moisture utilizing a ROSS Blender/Dryer?
This is possible depending on the material characteristics. The combination of vacuum, heat and proper agitation can accelerate drying time.
What is the difference between a single and double mechanical seal in an inline High Shear Mixer? When do I need to use one vs. the other?
The single mechanical seal is product-lubricated, so the product must have a good lubricating properties. When using a single mechanical seal, the mixer can never be run dry. In contrast the double mechanical seal utilizes a seal barrier fluid for lubrication. In general, the double mechanical seal performs better than a single when the product is a poor lubricant, contains abrasive particles, and/or occasionally runs dry.
What characteristics should I use/know when selecting a mixer for my process?
The most important characteristics to know to start the selection process would be:
- Batch size
- Viscosity range of the product during mixing process
- Product density
- Shear requirement or mixing intensity
How long do ROSS mixers last?
Service life depends on actual operating conditions but with proper maintenance, ROSS Mixers typically remain in service for many decades.
Does ROSS build custom-modified mixers?
Yes. We offer a wide range of mixers and blenders that are often customized for a particular process and application. Apart from our standard product lines, we also accept custom fabrication jobs including storage tanks, pressure vessels and reactors.
What attributes are assessed when scaling up?
When scaling up, the total amount of energy per unit of volume is taken into consideration. Other attributes such as tip speed, batch turnover, viscosity, and liquid rheology are also taken into consideration. Ross has over 180 years of experience assisting clients in all industries and frequently assists clients with the challenges of scaling up.
When are scrapers necessary?
The use of scrapers will depend on the product and process. Scrapers are beneficial when heating or cooling accompanies the mixing cycle. The use of scrapers in batch mixing helps improve product homogeneity and heat transfer efficiency. However, there are cases wherein scrapers are not recommended such as in the processing of abrasive applications or highly viscous, sticky materials.
Is it possible to overmix a product?
Yes. In order to determine the appropriate amount of mixing, the properties of the product should be well understood, which can be accomplished by testing and collecting data at various intervals. Overmixing is a broad term, covering a wide array of phenomena but ultimately refers to overworking a product beyond its final expected characteristics.
What are the considerations for integrating powder induction systems with high shear mixers?
Integrating powder induction systems with high shear mixers requires careful consideration of system compatibility, powder handling capabilities, and process requirements. Powder induction systems facilitate rapid dispersion of dry powders into liquid streams, enhancing mixing efficiency and reducing batch processing times. Choosing powder induction systems with adjustable powder feed rates, dust containment features, and compatibility with mixer configurations ensures seamless integration and consistent powder dispersion for various applications.
What role does temperature control play in optimizing mixing processes?
Temperature control can be critical in optimizing mixing processes as it often affects material viscosity, reaction rates, and product stability. Maintaining precise temperature conditions during mixing prevents thermal degradation of sensitive materials and can prevent vapor loss for products that benefit from processing at lower temperatures. Some products require processing at higher temperatures to adequately melt out components prior to dispersion. Utilizing mixers equipped with heating or cooling capabilities, along with automated temperature monitoring and control systems, ensures optimal process conditions and enhances overall mixing performance.
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Our Knowledge Center is full of insights and information towards how to blend different materials, which mixers are right for the job, and useful tips on setting up your production process line.